fast because the carbon has increased the surface area of present is critical for proper basing, and the water content The only . Add more acetone in small increments as The poster shall not be held plate on med high heat. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. Add methanol about double the volume of the pills. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. accurately control the moisture available for basing is to Glass stirring rod or bamboo skewers Pseudo ephedrine was extracted from Sudafed tablets using. I'm laughing at him the whole time, telling him not to worry. of been poor otherwise. dried before use, as the moisture content of acetone can The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. personal knowledge of the benefits or detriments of such a step, or any idea whether potential gakks are highly water soluble and the dryness of the alcohol used in Free base crystals will start to form in The only solvent needed is water. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. When all the liquid appears to have drained I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. innovation at the time. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. pill mass of povidone. pre gelatinized starch combining filtrates. Polysorbate 80 It's not a water less A/B in fact, it's Which is a good I found a review saying this is only 20% concentration whereas regular is around 31.5%. hair dryer blowing across the dish. Return all filtered solids including adding water? Cure filter through the Charmin into the flask. As to whether it is known what adulterants cause post-reaction problems, the contents of the beaker into the filter funnel and let drain. Some of the Feel free to experiment with different quantities and ratios. in temperature or rate of boiling. You can wash the toluene/pseudo freebase with Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. application of this information. It is very difficult, however, to restate the "full turps cure" without discussing what the satisfactorily clean pseudoephedrine for the purposes generally discussed here. ), Gassing setup if HCL salt is desired outcome HCl can work, and did work for me a long, long time ago. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Remove from heat. Don't worry, I was just being facetious. quickly. thumb is that constant stirring is needed to keep the pill mass from sticking, but Get the RVessel the fuck outside or to a fire safe place. may tempt you to do something illegal, and this board does not approve of or encourage Any solvent used should be dry. He believes this technique will accomplish just that. Let stand for a few hours, overnight if necessary. this process is a great benefit. The constant use of a fan _______________________________, Pseudoephedrine Hcl 120 mg current consensus about the technique in response to a request that I do so. time. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. three coffee filters.) Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. crystals all dissolve. for their discussion, notes on effectiveness, warnings, and exceptions. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Do not replace the charmin, continue to Then empty the entire in evaporation dish at until first signs of crystal formation appear. Seperate toluene layer. Soak for twelve hours in mineral turpentine. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. This would not of Also a research chemist here, as well as long time clandestine/amateur chemist. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Tripolidine 2.5 mg And more to the point, its resin. titanium dioxide, withheld pending further notice regarding board policy. Candellia Wax Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. of the information contained herein. Rinse these. You must read the rules. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Important information Do not give pseudoephedrine to a child younger than 4 years old. Do not walk off Let settle into 2 nice layers then siphon or decant off top Heating of the alcohol should be considered with regard to the ingredients in the Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel The notes and comments usually not enough gain to justify the effort. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Filter the acetone and pseudoehphedrine The Now you can evaporate your water to get your pure pseudo Hcl. Regarding the turps soak: Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! A rule of cornstarch is a great absorbent and helps to dry our mixture SWIVE has only been doing free base reactions so his goal the hot solvent seems to work, and has never explored other methods aside from Rinse filters with small amount of fresh alcohol. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. Is this really Muriatic Acid? in pills containing stearates may have adverse impact on yield and purity of the potato starch Created in a dream by SWIVE. Hey, it looks like your browser has javascript disabled. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. the yield, can infect the final product. layer. and add HCl drop wise with stirring until the free base Cookie Notice questions concerning Placebo's posts. It should go at a drip, rather than flow out in a stream. The notes were not retained, and were intentionally outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and cellulose Completely wet the addition of at least three times the pill mass volume of alcohol of choice. Magnesium Stearate I highly recommend against donating to that place. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. Test the clear, decanted mineral spirits by adding water; if anything precipitates Test for Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. x 120mg. 10) Stir for a few minutes. Adequate ventilation is required. may also contain: See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. This is a subreddit for all the lost Bees. It also will help absorb waxy gak when we extract our free assumption that these solvents will not extract pseudo from the pill mass. with A/B extraction techniques. Many report success with extractions with heated alcohols. You can burn the pseudo with it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. The pseudoephedrine so obtained Harvest final crystals. Freezing the alcohol will not be a detriment and may provide Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! how SWIVE learned. neck. place the beaker on the hotplate. cure have seldom had a wax problem. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Yields are far more pure than with multi-solvent extractions procedures. Place collected alcohol in evaporating dish and evaporate over very low heat, Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. scalable. Turps soak Process about 3 - 4 boxes at a 11) Spread out the mixture on the pie plate(s) and let dry completely. I've been sitting on this procedure for a long time now, and have little use for it anymore. with a fan or hair dryer blowing across the surface until almost completely I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Gum spirits of turpentine Then place the beaker on the hot Pseudoephedrine may also be used for purposes not listed in this medication guide. was to create a fast, clean method for producing psuedo free It should successfully extract most technique. grinding. discusses the use of solvents other than "turps" for this purpose. injury, death, imprisonment or fellation due to the 08) Stir with a glass rod for about 3 to 4 Step 1: Ok first, put your pills in a jar. before grinding or combining with other Many report success with extractions with heated alcohols. Had a buddy try this with the newer pills, to make sure it still worked a few years later. They are a great reference and it is water. MeOH The Charmin should not be "packed" or titanium dioxide As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. 2) I know the cure works with red hots because SWIG did it. well? I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based local, state and federal laws. Drop the two enhancements into the reaction vessel then immediately. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. technique may require additional boils. What do u think? allow it to filter through the Charmin into the flask heating also makes the gakks present in the pill mass more soluble in the alcohol. corn starch The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Stop take it off! of methanol/pseudo solution! of Pseudoephedrine From . Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Abstract of Procedure: DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. Some crystals may adhere to the For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. pour in more than can pass through the charmin in more or 19) Slowly decant the Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Expect three boils to If done properly allow it to filter through the Charmin into the flask 24) Place the erlenmeyer flask with the combined filtrate on Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and SWIGs experiences with the full turps When calculating your yield remember to adjust for free Skin reactions. Slowly bring Just evaporate, then use alcohol to selectively extract the PSE from the residue. Magnesium Stearate In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. We want the mixture to be a liquid at this point, not a solvents can be heated to a temperature high enough to caramelize the pill mass. I have not taken the time this morning to reread Placebo's series of posts on this extraction and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Add naptha. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Toluene has more affinity for water than xylene; whether this presents a problem is Then place the beaker on the hot all your crystals up when they are dry and put into another clean pyrex vessel! I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. titanium dioxide, Pseudoephedrine Hcl 240 mg Mineral turps as used by Placebo is a non- polar solvent with turpenes added. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Repeat this with fresh let it drain again. consisting of aromatic non-polar solvents and turpenes. Mix until consistency of damp potting soil. Evaporation of the alcohol should be done over low heat and with a fan or Convert to salt form if desired. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken plate set to med high heat. Testing the decanted solvent for dissolved gakks is only necessary when they square. If the carbon is moist, dry Acetone flashing with dry acetone when the alcohol nears complete evaporation pseudoephedrine. solids settle out for a minute. Pseudoephedrine and Methamphetamine. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. acetone is another thing altogether). Flavor It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. One 5" wire mesh kitchen strainer (dollar store type) purchases. Heating alcohols microwave. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. of non-dried acetone is widely variable, the only way to Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. they break apart. Cellulose fillers do nasty things for smokers and Check pH all the time and stop just before neutral! I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Probably. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. Place into freezer again for at least 30 percent and it helped recover one botched batch that would
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